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This bromo ketone is reacted with ethanolic methylamine to provide the 3-MMC free base , which might be remodeled for the hydrochloride salt (VI) by addition of ethereal hydrogen chloride.
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02 Feb #5 If he made use of acidification with water and DCM, then he divided h2o layer with four-MMC*HCl after which washed this layer with DCM various instances. Just after which you could leave it in container for crystallization. Just my feelings. Is usually various from his system.
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